CHEM 3560 - Molecular Structure Determination III

North Terrace Campus - Semester 1 - 2020

Chemical structure determination techniques underpin much of the work carried out in research, analytical, and industrial laboratories. This course provides the student with an in-depth understanding of the most significant molecular structure determination techniques, including X-ray crystallography, X-ray spectroscopy, scanning and transmission electron microscopy and associated microanalysis, advanced nuclear magnetic resonance (NMR) and electron paramagnetic resonance (EPR) spectroscopy, advanced electronic and vibrational spectroscopy including Raman and circular dichroism spectroscopy, and biological structure determination by mass spectrometry. Hands-on practical experience with these techniques is emphasised, through extensive workshop and laboratory activities.

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Course Details

Course Code	CHEM 3560
Course	Molecular Structure Determination III
Coordinating Unit	School of Physical Sciences
Term	Semester 1
Level	Undergraduate
Location/s	North Terrace Campus
Units	6
Contact	Up to 12 hours per week
Available for Study Abroad and Exchange	Y
Prerequisites	CHEM 2510 and CHEM 2520
Corequisites	CHEM 3111 or equivalent
Assessment	Final examination, workshop/practical assignments, presentations

Course Staff

Course Coordinator: Associate Professor David Huang

Course Timetable

The full timetable of all activities for this course can be accessed from .

Course Learning Outcomes

1	Describe and explain the physical and chemical principles that underlie molecular structure determination techniques such as X-ray and spectroscopy, electron and scanning probe microscopy, NMR and EPR spectroscopy, electronic and vibrational spectroscopy, and mass spectrometry.
2	Apply knowledge of molecular structure determination techniques to identify and/or characterise chemical compounds from experimental data.
3	Devise solutions to chemical structure determination problems by integrating information from a variety of techniques.
4	Assess the appropriateness of different structure determination techniques for solving particular structure determination problems.
5	Critically analyse the application of molecular structure determination techniques in research journal articles and effectively communicate these findings in oral presentations.
6	Conduct, analyse, and interpret results of an experiment, and effectively communicate these in written reports.

University Graduate Attributes

This course will provide students with an opportunity to develop the Graduate Attribute(s) specified below:

University Graduate Attribute	Course Learning Outcome(s)
Deep discipline knowledge informed and infused by cutting edge research, scaffolded throughout their program of studies acquired from personal interaction with research active educators, from year 1 accredited or validated against national or international standards (for relevant programs)	1-6
Critical thinking and problem solving steeped in research methods and rigor based on empirical evidence and the scientific approach to knowledge development demonstrated through appropriate and relevant assessment	2-6
Teamwork and communication skills developed from, with, and via the SGDE honed through assessment and practice throughout the program of studies encouraged and valued in all aspects of learning	5-6
Career and leadership readiness technology savvy professional and, where relevant, fully accredited forward thinking and well informed tested and validated by work based experiences	1-6
Intercultural and ethical competency adept at operating in other cultures comfortable with different nationalities and social contexts able to determine and contribute to desirable social outcomes demonstrated by study abroad or with an understanding of indigenous knowledges	5-6
Self-awareness and emotional intelligence a capacity for self-reflection and a willingness to engage in self-appraisal open to objective and constructive feedback from supervisors and peers able to negotiate difficult social situations, defuse conflict and engage positively in purposeful debate	5-6

Learning Resources

Required Resources

There is no prescribed text for this course.

Recommended Resources

Maths Resources

The Maths Learning Centre (MLC) helps all students learn and use the maths they need at uni. The MLC offers seminars, workshops, online, and print resources. It also run a drop-in room in Hub Central from 10am to 4pm Monday to Friday during teaching weeks. For more information, visit

For chemistry-specific maths help, visit

Online Learning

MyUni: Teaching materials and course documentation will be posted on the MyUni website (http://myuni.adelaide.edu.au/).
Learning & Teaching Activities

Learning & Teaching Modes

This course will be delivered by the following means:

· Lectures 24 x 2-hour sessions with 2 sessions per week

· Workshops 12 x 3-hour sessions with 1 session per week

· Practicals 6 x 6-hour sessions with 1 session per fortnight

· Presentations 2 x 5-hour sessions during the semester

Workload

The information below is provided as a guide to assist students in engaging appropriately with the course requirements.

A student enrolled in a 6 unit course, such as this, should expect to spend, on average 24 hours per week on the studies required. This includes both the formal contact time required to the course (e.g., lectures and practicals), as well as non-contact time (e.g., reading and revision).

Learning Activities Summary

Lectures

Lectures will be used to convey the theoretical basis of the molecular structure determination techniques that will be explored in the workshops and practicals.

Workshops

Workshops will be used to reinforce the concepts introduced in lectures through a combination of quantitative problem solving, a discussion of the operational principles, including the strengths and weaknesses of various structure determination methods, and consideration of appropriate possible solutions to chemical structure determination problems.

Practicals
Practical exercises will provide students with “hands on” experience in the quantitative use of various analytical methods. In addition, students will be involved in the analysis of “real world” chemical samples.

Specific Course Requirements

Attendance is compulsory at all scheduled chemistry practical sessions. The learning outcomes for this course are substantially dependent on laboratory experience and practice. Therefore, missing any practical class in a semester will result in a grade of FAIL being recorded for the course.

Small Group Discovery Experience

Each of the 12 weekly workshops will be led by an experienced academic and will involve the students working in small groups of 2−4 to solve molecular structure determination problems using primary data provided by the academic. The workshop activities will require students to engage actively with the course material to arrive at solutions to complex chemical structure problems in a process that mirrors the process of discovery in research.

The University's policy on Assessment for Coursework Programs is based on the following four principles:

Assessment must encourage and reinforce learning.
Assessment must enable robust and fair judgements about student performance.
Assessment practices must be fair and equitable to students and give them the opportunity to demonstrate what they have learned.
Assessment must maintain academic standards.

Assessment Summary

Due to the current COVID-19 situation modified arrangements have been made to assessments to facilitate remote learning and teaching.
Assessment task	Type of assessment	Percentage of total assessment for grading purposes	Hurdle Yes or No	Outcomes being assessed / achieved	Approximate Timing of Assessment
Workshop/practical assignments	Formative & Summative	48%	No	1 –4, 6	Every two weeks
Presentations	Summative	10%	No	5	Week 13
Examination	Summative	42%	Yes	1–4	End-of-semester examination period

Assessment Related Requirements

Practical work is compulsory – This includes attendance, conduct of required experimental work, attendance at demonstrator interviews (as required) and submission of laboratory reports. The learning outcomes for this course are substantially dependent on laboratory experience and practice. Therefore, missing any practical class in a semester will result in a grade of FAIL being recorded for the course. Students with medical or compassionate reasons for non-attendance will be given an opportunity to make up missed practical sessions.

To pass this course, students must attain a minimum of 45% for the examination and attend all practicals. Students who attain a final course grade of at least 45% but do not attain a minimum of 45% for the exam may be offered an Additional Academic Exam during the Replacement/Additional Assessment period, in line with the Modified Arrangements for Coursework Assessment Policy.

Assessment Detail

Workshop/practical assignments (48%)

Students will complete 2 workshop sessions for each of the 6 modules in the course and 1 practical session or practical-related online activity for each course module except the Electron and Scanning Probe Microscopy module. For each module, they will complete an assignment or assignments in which they discuss the results of experiments carried out in the practical session and data analysis undertaken in the workshop sessions, as well as answer specific questions related to the techniques used in the workshops and practical. The assessment for each module will be 9% of the course grade, except for the X-ray Crystallography and Electron and Scanning Probe Microscopy modules, for which the assessment will be 8% and 4% of the course grade, respectively. Practicals are compulsory and students must attend all practicals. If students do not meet the attendance requirement for practicals they will receive a Fail Grade. There is the opportunity for students to make up missed practicals.

Presentations (10%)

Each student will give one 10-minute oral presentations online via Zoom (plus 3 minutes for questions) in which the student will be required to critically analyse the application of a molecular structure determination technique in a research journal article. The two presentations must be on a distinct technique covered in the course.

Examination (42%)

The final examination will examine all components of the course. It will consist of multiple-choice, short-answer and long-answer questions. Students must achieve a minimum overall mark of 45% for the examination component to pass the course.

Submission

Late Submission

If an extension is not applied for, or not granted then a penalty for late submission will apply. A penalty of 10% of the value of the assignment for each calendar day that the assignment is late (i.e. weekends count as 2 days), up to a maximum of 50% of the available marks will be applied. This means that an assignment that is 5 days late or more without an approved extension can only receive a maximum of 50% of the marks available for that assignment.

Course Grading

Grades for your performance in this course will be awarded in accordance with the following scheme:

M10 (Coursework Mark Scheme)
Grade	Mark	Description
FNS		Fail No Submission
F	1-49	Fail
P	50-64	Pass
C	65-74	Credit
D	75-84	Distinction
HD	85-100	High Distinction
CN		Continuing
NFE		No Formal Examination
RP		Result Pending

Further details of the grades/results can be obtained from Examinations.

Grade Descriptors are available which provide a general guide to the standard of work that is expected at each grade level. More information at Assessment for Coursework Programs.

Final results for this course will be made available through .

Student Feedback

The University places a high priority on approaches to learning and teaching that enhance the student experience. Feedback is sought from students in a variety of ways including on-going engagement with staff, the use of online discussion boards and the use of Student Experience of Learning and Teaching (SELT) surveys as well as GOS surveys and Program reviews.

SELTs are an important source of information to inform individual teaching practice, decisions about teaching duties, and course and program curriculum design. They enable the University to assess how effectively its learning environments and teaching practices facilitate student engagement and learning outcomes. Under the current SELT Policy (http://www.adelaide.edu.au/policies/101/) course SELTs are mandated and must be conducted at the conclusion of each term/semester/trimester for every course offering. Feedback on issues raised through course SELT surveys is made available to enrolled students through various resources (e.g. MyUni). In addition aggregated course SELT data is available.
Student Support
Policies & Guidelines
This section contains links to relevant assessment-related policies and guidelines - all university policies.
Fraud Awareness

Students are reminded that in order to maintain the academic integrity of all programs and courses, the university has a zero-tolerance approach to students offering money or significant value goods or services to any staff member who is involved in their teaching or assessment. Students offering lecturers or tutors or professional staff anything more than a small token of appreciation is totally unacceptable, in any circumstances. Staff members are obliged to report all such incidents to their supervisor/manager, who will refer them for action under the university's student鈥檚 disciplinary procedures.

The 成人大片 is committed to regular reviews of the courses and programs it offers to students. The 成人大片 therefore reserves the right to discontinue or vary programs and courses without notice. Please read the important information contained in the disclaimer.

Authorised by:	Deputy Vice-Chancellor and Vice-President (Academic)
Maintained by:	Course Outlines Administrator

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